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  • Application Note

    Analysis of Single-Walled Carbon Nanotubes with SP-ICP-MS

    Measuring the amount of metals in CNTs presents a challenge. High levels can be measured directly in the solid by several techniques, including XRF and TEM, while low-level analysis requires complete digestion of the sample prior to analysis by ICP-OES or ICP-MS.

  • Flyer

    OilPrep 4 Oil Diluter Flyer

    Need flexible sample preparation for wear metals and particle count analyses? The OilPrep? 4 is a dedicated four-tip oil diluter that automatically dilutes oil samples with kerosene (V-Solv? ICP solvent), in preparation for wear metals and particle counting/sizing analyses by inductively coupled plasma (ICP-OES) and single particle optical sizing (SPOS), such as with the Avio? ICP-OES and LPC 500? Liquid Particle Counter.

    Some key benefits include:

    • • High throughput – Significantly improves productivity and efficiency versus manual or single-tip systems. Diluting up to 250 samples per hour, one OilPrep 4 oil diluter can prepare approximately 2000 samples in 8 hours.
    • • Flexibility – Innovative Varispan? technology provides automatic computer-controlled variable sample probe spacing for multi-tipped processing of original sample containers.
    • • Time Savings – Unlike alternate technologies, PerkinElmer’s Ultrasonic Liquid Level Sensing is not impacted by individual sample viscosities, color, or external lighting.

    Download the flyer to discover more.

  • White Paper

    Weighing the Benefits and Risks of Nanotechnology White Paper

    There is a growing body of evidence showing that there are significant differences between some nanomaterials and their non-nanoscale counterparts. What those differences portend raises many new questions about their potential to cause harm to human health and the environment.

  • White Paper

    An Introduction to Single Cell ICP-MS Analysis

    In this white paper, we will introduce the concept of Single Cell ICP-MS (SC-ICP-MS), where individual cells are rapidly analyzed for metal content.

    Research into the effectiveness of anti-cancer medications is explored by monitoring the uptake rate of cisplatin at the cellular level, advancing the knowledge of cellular interactions with metal-containing species. SC-ICP-MS allows users to monitor metal content within single cells for intrinsic metal content, uptake of ionic and/or nanoparticulate contaminants, handle lower cell numbers compared to conventional methods, and use minimal sample preparation.

  • Application Note

    Analysis of Drinking and Natural Waters using the NexION 2000 ICP-MS

    This work has demonstrated the ability of the NexION 2000 ICP-MS to analyze both natural and drinking water samples in Standard (i.e. non-cell) mode, in accordance with U.S. EPA Method 200.8. Accuracy has been demonstrated through the analysis of several reference materials and spike recoveries, with stability of at least nine hours. Method detection limits allow for trace-level determinations, while the ability to selectively suppress user-defined isotopes also allows the measurement of analyte levels usually only possible by ICP-OES or Flame AA. The NexION 2000 provides a comprehensive solution to the challenge of U.S. EPA Method 200.8 and other drinking and natural water analytical requirements across the globe.

  • Application Note

    Testing and Validation of Various Antacids for Elemental Impurities using the NexION 2000 ICP-MS

    The United States Pharmacopeia (USP) has announced that its new standards for elemental impurities in drug products has been implemented since January 1, 2018. General Chapters <232> and <2232> specify the list of elements and their permissible daily exposure (PDE) limits based on the route of administration.

  • Application Note

    Quantification of Nanoparticle Uptake into Cancer Cells using Single Cell ICP-MS

    Nanoparticles (NPs) have been of significant interest over the last two decades as they offer attractive benefits for drug delivery to overcome limitations in conventional chemotherapy. Nanoparticles can be engineered to carry both drugs and imaging probes to simultaneously detect and treat cancer. They may also be designed to specifically target diseased tissues and cells in the body. A number of nanoparticlebased cancer therapeutics have been approved for clinical use and/or are currently under development.

  • Case Study

    PerkinElmer and Missouri S&T Collaborate on Nanoparticle Study

    As with any new field of study, nanotechnology and the creation of ENPs may pose unintended environmental, health, and safety risks demanding further study. The traditional research process involving nanomaterials, however, requires many different types of technologies, including electron microscopes, great technical expertise, hours of manual calculations, and considerable investments in research to obtain a single piece of information.

  • Application Note

    Ultratrace Interference-Free Analysis of Solar-Grade Silicon Wafers by ELAN DRC II ICP-MS

    A new, simple sample-preparation method which results in minimal contamination has been developed for the ultratrace interference-free analysis of solar-grade silicon wafers using an ELAN DRC II ICP-MS.

  • Case Study

    Colorado School of Mines Uses a NexION 300Q ICP-MS to Obtain a Better Understanding of the Environmental Impact of Engineered Nanomaterials

    One of the leading academic research groups involved with the study of the impact of ENPs on the environment is the Colorado School of Mines (CSM), based in Golden, Colorado.

  • Application Note

    Microwave Digestion - EPA Method 3052 on the Multiwave 3000

    Microwave sample preparation provides an efficient and clean sample preparation for multi-element analytical techniques such as ICP-OES and ICP-MS. As Microwave assisted digestion has evolved, so have the methodologies. EPA method 3052 is designed for the “total” analysis in a variety of matrices including soil, sediments, sludge, oils, biological and botanical materials. This method is the most versatile and has been well proven. It allows variations in reagents and methodology, making it ideal for a variety of matrices and elements. The variability of this method also requires a basic understanding of digestion chemistry.

  • Application Note

    Meeting the Challenges of Soil Analysis with the Avio 200 ICP-OES

    The analysis of soils for elemental contents presents challenges during the sample preparation step. A common method for preparing a soil sample for inorganic elemental analysis involves digesting the soil sample in an acid that is heated to near-boiling to extract the elements for analysis. When using open vessels in heating blocks, this extraction method typically takes four hours or more to complete. The sample must then be centrifuged or filtered to remove solid particles prior to analysis. The use of a microwave digestion system can speed this up significantly by completing the acid digestion in less than 50 minutes.

  • Application Note

    Impurities in Lead with the Avio 500 ICP-OES Following London Metal Exchange Guidelines

    The London Metal Exchange issues specifications for a number of different metals in several grades. This work focuses on the analysis of lead of different purities with PerkinElmer’s Avio? 500 ICP Optical Emission Spectrometer (ICP-OES), using “Special Contract Rules for Standard Lead1” as a guideline for the analytes and concentrations.

  • Application Note

    Accurate Sizing and Precise Counting of 10 nm Gold Nanoparticles using the NexION 2000 ICP-MS

    In this work, we demonstrate that PerkinElmer's NexION? 2000 ICP-MS, with its unique RF generator and ion optics, coupled with the Syngistix? Nano Application Software Module, can be used to accurately measure and characterize NP sizes of 10 nm and smaller, both alone and in a mixture of NPs of various sizes.

  • Application Note

    Analysis of Cerium Dioxide Nanoparticles in Soil Using Single Particle ICP-MS

    This work demonstrates a robust method using SP-ICP-MS technology to detect CeO2 NPs which were extracted from soil samples with tetrasodium pyrophosphate (TSPP). Over the past few decades, engineered nanoparticles (ENPs) have been increasingly used in many commercial products. As a result, more and more ENPs have been released into the environment, which raises concerns over their fate, toxicity and transport therein.

  • Application Note

    Analysis of Oil Additives Following ASTM D4951 with the Avio 200 ICP-OES

    When blending base oils and additives for use as lubricants, it is important to know and control the concentrations of certain elements for optimal performance and longer engine life. This work will focus on the analysis of additives in new oils using PerkinElmer’s Avio? 200 ICP Optical Emission Spectrometer (ICP-OES), which overcomes limitations of other ICP-OES systems and X-ray analyses.

  • Application Note

    The Determination of Lead in Calcium-Based Antacid and Dietary Supplements Using the NexION 350 ICP-MS System to Comply with the State of California's Proposition 65 Legislation

    Compliance with California’s Proposition 65 for the monitoring of lead (Pb) in calcium-based antacid medications and dietary supplements requires the analytical methodology to demonstrate detection limits below 0.05 μg/g in the solid material. The analytical capabilities of Inductively Coupled Plasma Mass Spectrometry (ICP-MS) make it the most suitable technique for performing lead determinations at these low levels on a routine basis.

  • Brochure

    OilExpress 4 Oil Condition Monitoring System

    The OilExpress 4 system adapts to your laboratory’s needs, from dozens to thousands of samples per day. Its modular design makes it possible to scale up your sample throughput or separately utilize the oil dilution capabilities in busy laboratories that are using ICP analysis. The system minimizes your operational costs by reducing instrument downtime, increasing throughput to reduce cost per sample, and offering significant savings from decreased solvent waste.

  • Application Note

    Using MSF to Resolve Difficult Interferences in Metallurgical Samples with the Avio 500 ICP-OES

    The analysis of trace metals in metallurgical matrices also presents a challenge for ICP-OES: spectral interferences. Many elements have a large number of emission lines (i.e. approximately 20,000 for iron), which increases the potential for spectral interferences. This effect is compounded in metallurgical samples, where the matrix element(s) are present at high levels due to the minimal dilutions used.

  • Application Note

    Characterization of TiO2 Nanoparticle Release from Fabrics By Single Particle ICP-MS

    In the textile industry, the use of titanium dioxide (TiO2) nanoparticles (NPs) is increasing due to their ability to provide UV protection, increase the hydrophilic nature of fabrics, provide antibacterial characteristics, and reduce odors. This work demonstrates the ability of PerkinElmer's NexION® Single Particle ICP-MS with Syngistix Nano Application Software Module to both detect and measure TiO2 nanoparticles released from textiles.

  • White Paper

    Single Particle Inductively Coupled Plasma Mass Spectrometry: Understanding How and Why

    Analyzing single nanoparticles with ICP-MS requires a different approach than measuring dissolved elements. This work describes the theory behind single-particle ICP-MS measurements, drawing comparisons and differences with analyzing dissolved elements.

  • Application Note

    Analysis of Soils and Waters in Accordance with U.S. EPA Method 6020B using the NexION 2000 ICP-MS

    Through the years, both industry and analytical instrumentation have advanced. With the development of new chemicals and processes, new pollutants may enter the environment. However, the capabilities of analytical instruments have also increased, allowing the measurement of ever lower levels of environmental contaminants, as well as new pollutants.

  • Flyer

    NexSAR HPLC-ICP-MS Speciation Solution

    Speciation studies can provide comprehensive information regarding ion mobility, bioavailability, and toxicity. Consequently, many modern labs are expanding their analytical portfolio to include HPLC-ICP-MS. For such studies, it is advantageous to have an intuitive, user-friendly system that meets the user requirements for automation, ultra-low baseline, powerful integration, and flexible data export. And no one offers a more integrated, versatile, and inert speciation solution than PerkinElmer - accelerate your speciation analysis with the NexSAR? HPLC-ICP-MS Speciation Solution.

  • Application Note

    Analysis of Impurities in Nickel with Avio 500 ICP-OES Following London Metal Exchange Guidelines

    The London Metal Exchange (LME) issues specifications for a variety of purities for different metals. This work focuses on the analysis of contaminants in nickel with PerkinElmer’s Avio? 500 ICP Optical Emission Spectrometer (ICP-OES), using “Special Contract Rules for Primary Nickel” as a guideline for the analytes and required concentrations.

  • Application Note

    Analysis of In-Service Oils Following ASTM D5185 with the Avio 500 ICP-OES

    Globally, heavy machinery is used in construction, mining, and a variety of other areas. As the scale of the operations increase, the size, complexity, and cost of the equipment also increase, meaning that breakdowns can be costly, both in equipment repair and lost revenue. As a result, preventive maintenance is paramount. Lubricants are among the key fluids that can be tested, especially the oil used in engines. By monitoring the elemental concentration of the oil or other lubricants (hydraulics, transmission, gear), the status of that compartment can be determined.

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